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INTERNATIONAL JOURNAL OF CREATIVE RESEARCH THOUGHTS - IJCRT (IJCRT.ORG)
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ISSN Approved Journal No: 2320-2882 | Impact factor: 7.97 | ESTD Year: 2013
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Paper Title
Crystal structures of two homologues: diethyl (benzo[d][1,3]dioxol-5-yl((4-bromophenyl)amino)methyl)phosphonate and dibutyl(benzo[d][1,3] dioxol-5-yl((4-bromophenyl)amino)methyl)phosphonate
Authors
KodagalaKameswara Rao, Dr. R. Raja, Mat�as Ignacio Castillo Opazo, Ester Antonia Herrera Caro, Roc�o Carolina Gallardo Rivera, NemallapudiBakthavatchalaReddy, MusaliKrishnaiah
Keywords
single-crystal X-ray study; T = 296 K; mean (C-C) = 0.006 A?; R-factor = 0.0550 in I and 0.0699 in II; wR factor = 0.1429 in I and 0.1869 in II; data-to-parameter ratio 25.9.
Abstract
The title compounds, C18H21BrNO5P (I) and C22H29BrNO5P (II) form a homologous series, the structures determinations confirm the nature of the products. The compounds all crystallize in Space group C2/c for compound I and P-1for compound II. Differ by the presence of a Phosphonate atom instead of a dibutyl atom in the para position of two benzo atom of compound (II). Bond lengths and angles may be considered normal for these compound types. The dioxole rings in both structures similar planar conformations. Intra- and Intermolecular C-H...O and N-H...O hydrogen bonds are responsible for the consolidation of the crystal packing of both molecules. In addition to this, weak C-H...? interactions are also observed.
IJCRT's Publication Details
Unique Identification Number - IJCRT23A5051
Paper ID - 237955
Page Number(s) - i604-i609
Pubished in - Volume 11 | Issue 5 | May 2023
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Publisher Name - IJCRT | www.ijcrt.org | ISSN : 2320-2882
E-ISSN Number - 2320-2882
Cite this article
KodagalaKameswara Rao, Dr. R. Raja, Mat�as Ignacio Castillo Opazo, Ester Antonia Herrera Caro, Roc�o Carolina Gallardo Rivera, NemallapudiBakthavatchalaReddy, MusaliKrishnaiah, "Crystal structures of two homologues: diethyl (benzo[d][1,3]dioxol-5-yl((4-bromophenyl)amino)methyl)phosphonate and dibutyl(benzo[d][1,3] dioxol-5-yl((4-bromophenyl)amino)methyl)phosphonate", International Journal of Creative Research Thoughts (IJCRT), ISSN:2320-2882, Volume.11, Issue 5, pp.i604-i609, May 2023, Available at :http://www.ijcrt.org/papers/IJCRT23A5051.pdf
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ISSN: 2320-2882 Impact Factor: 7.97 and ISSN APPROVED Journal Starting Year (ESTD) : 2013
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ISSN: 2320-2882 Impact Factor: 7.97 and ISSN APPROVED Journal Starting Year (ESTD) : 2013
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