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INTERNATIONAL JOURNAL OF CREATIVE RESEARCH THOUGHTS - IJCRT (IJCRT.ORG)
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ISSN Approved Journal No: 2320-2882 | Impact factor: 7.97 | ESTD Year: 2013
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Published Paper Details:
Paper Title
ANALYTICAL METHOD DEVELOPMENT AND VALIDATION STUDIES OF ANTI DIABETIC DRUGS BY HPLC.
Authors
Pallavi Hade, Raman R. Chandak
Keywords
KEYWORDS: - Metformin hydrochloride, Teneligliptin, HPLC, Pharmaceutical dosage forms.
Abstract
ABSTRACT:
A simple, sensitive and high performance liquid chromatographic method was developed for the estimation of anti-diabetic drugs Metformin Hydrochloride (MET) and Teneligliptin (TEN) in pure and in pharmaceutical dosage forms. A Gemini C18 column (150x4.6mm, 5?) was used with a mobile phase contain a mixture of Ammonium Acetate Buffer (pH-3) and Acetonitrile taking ratio of 42: 58. Set the flow rate was 0.3ml/min and effluents were monitored at 255nm and eluted at 5.18min (MET) and 8.1min (TEN). Calibration curve was plotted within range from 0.5-51 ?g/ml for MET and 0.3-31 ?g/ml for TEN. This assay was validated for the parameters i.e. accuracy, precision, robustness and all system suitability parameter. The method can be useful routine analysis for the determination on metformin and teneligliptin in pharmaceutical dosage forms.
IJCRT's Publication Details
Unique Identification Number - IJCRT2111092
Paper ID - 212546
Page Number(s) - a740-a745
Pubished in - Volume 9 | Issue 11 | November 2021
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Publisher Name - IJCRT | www.ijcrt.org | ISSN : 2320-2882
E-ISSN Number - 2320-2882
Cite this article
Pallavi Hade, Raman R. Chandak, "ANALYTICAL METHOD DEVELOPMENT AND VALIDATION STUDIES OF ANTI DIABETIC DRUGS BY HPLC.", International Journal of Creative Research Thoughts (IJCRT), ISSN:2320-2882, Volume.9, Issue 11, pp.a740-a745, November 2021, Available at :http://www.ijcrt.org/papers/IJCRT2111092.pdf
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ISSN: 2320-2882 Impact Factor: 7.97 and ISSN APPROVED Journal Starting Year (ESTD) : 2013
ISSN and 7.97 Impact Factor Details
ISSN: 2320-2882 Impact Factor: 7.97 and ISSN APPROVED Journal Starting Year (ESTD) : 2013
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