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  Published Paper Details:

  Paper Title

SYNTHESIS & CHARACTERIZATION OF COPPER OXIDE (CU2O) AND COPPER SULPHIDE (CU2S) NANOPARTICLES USING XRD ANALYSIS

  Authors

  Ankur

  Keywords

Nanomaterials, Solids, strength, enormous, contrasted, transformation, PPS, self-quenching, XRD , TEM analysis.

  Abstract


Nano-materials can be characterized as solids having measurements in the nanometer system. So, nanomaterials structure a unique class of materials that lie in the area that is in the middle of two limits i.e. mass solids and atoms. Solids and atoms have been contemplated and seen very well, anyway nanomaterials show properties that are totally not the same as both of the two. The properties of these materials are described by a particular length scale, normally underneath ~ 100 nm. In the event that the actual size of the material is decreased underneath this length scale, it's all properties like mechanical, strength, warm, optical, attractive, directing and so forth changes and become touchy to its size and shape. The purpose behind the variety in properties with size of the materials originates from very enormous surface-to-volume proportion. As such, nanomaterials have enormous number of particles on their surface when contrasted with those in the inside. Nanoscale metals/metal oxides/metal sulfides show electro-optical and mechanical properties that are not quite the same as their mass partners are promising materials for a few innovative applications, for example, photograph warm transformation, catalysis, sensors and so forth. In this present paper , an effort is there to explain the utilization of polymer inorganic strong state response course towards the union of copper (Cu), copper oxide (CuO), and copper sulfide (Cu2S) nano-particles. We endeavored the responses utilizing 1:1, 1:5, 1:10, 1:15 & 1:20 molar proportions of the copper salts, copper acetic acid derivation [Cu(CH3COO)2:H2O], copper chloride (CuCl2), copper carbonate (CuCO3), and copper nitrate [Cu(NO2)2] and polymer, Polyphenelene sulfide [1/n[C6H4S]n, (PPS)]. The PPS was picked intentionally in light of the fact that it is designing thermoplastic polymer having astounding mechanical and substance opposition properties notwithstanding the polymer being inalienably self-quenching. For these responses, the two reactants were admixed in the molar proportions in an agate pastel-mortar by utilizing CH3)2CO. The resultant admixture was warmed at 2850C (dissolving temperature of PPS) in an alumina pot for 6 hours under a surrounding climate condition. The combined items were portrayed by different physicochemical methods like XRD and TEM analysis. The example relating to warmed admixtures of various [Cu (CH3COO)2 H2O]:PPS proportions obviously shows transcendence of the development of copper sulfide (Cu2S) stage in equi-molar proportion samples. The samples arranged at other molar proportions show presence of metallic copper with some copper oxide stage present in it. The item integrated from copper nitrate [Cu(NO2)2] can frame copper sulfide (Cu2S), when responded with Polyphenelene sulfide (PPS). The copper carbonate (CuCO3) surrender copper inadequate construction Cu1.96S though copper chloride (CuCl2) remains un-reacted for certain hints of Cu1.96S. The future extent of the current work can be expected by examining the viewpoints of novel polymer-inorganic strong state responses for the amalgamation of other inorganic salts and its extension for the expected applications.

  IJCRT's Publication Details

  Unique Identification Number - IJCRT2103314

  Paper ID - 204573

  Page Number(s) - 2522-2528

  Pubished in - Volume 9 | Issue 3 | March 2021

  DOI (Digital Object Identifier) -   

  Publisher Name - IJCRT | www.ijcrt.org | ISSN : 2320-2882

  E-ISSN Number - 2320-2882

  Cite this article

  Ankur,   "SYNTHESIS & CHARACTERIZATION OF COPPER OXIDE (CU2O) AND COPPER SULPHIDE (CU2S) NANOPARTICLES USING XRD ANALYSIS", International Journal of Creative Research Thoughts (IJCRT), ISSN:2320-2882, Volume.9, Issue 3, pp.2522-2528, March 2021, Available at :http://www.ijcrt.org/papers/IJCRT2103314.pdf

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